6H4A
Human MALT1(329-728) in complex with MLT-748
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-04-29 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 94.930, 68.930, 56.750 |
| Unit cell angles | 90.00, 92.65, 90.00 |
Refinement procedure
| Resolution | 47.410 - 2.650 |
| R-factor | 0.192 |
| Rwork | 0.190 |
| R-free | 0.24000 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 3v55 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.210 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.410 | 2.660 |
| High resolution limit [Å] | 2.650 | 2.650 |
| Rmerge | 0.073 | 0.768 |
| Number of reflections | 10676 | |
| <I/σ(I)> | 9 | 1.6 |
| Completeness [%] | 99.5 | 100 |
| Redundancy | 3.3 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | PEG 2000 0.1M Mes pH 6.5 |
