6GY7

Crystal structure of XaxB from Xenorhabdus nematophil

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-02-24
Detector	PSI PILATUS 6M
Wavelength(s)	0.97793
Spacegroup name	P 21 21 21
Unit cell lengths	88.700, 99.410, 194.150
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.537 - 3.400
R-factor	0.2657
Rwork	0.264
R-free	0.30450
Structure solution method	SAD
RMSD bond length	0.004
RMSD bond angle	0.714
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	CRANK2
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.490
High resolution limit [Å]	3.400	3.400
Number of reflections	45577
<I/σ(I)>	10.36
Completeness [%]	100.0
Redundancy	21.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	293.15	0.2 M NaBr, 0.1 KCl, 20 % PEG 3350