6GPL
Crystal structure of human GDP-D-mannose 4,6-dehydratase in complex with GDP-4k6d-Man
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 89.260, 122.770, 139.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.090 - 1.760 |
R-factor | 0.16962 |
Rwork | 0.169 |
R-free | 0.18956 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.464 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.090 | 1.810 |
High resolution limit [Å] | 1.760 | 1.760 |
Number of reflections | 151973 | |
<I/σ(I)> | 13.3 | 1.4 |
Completeness [%] | 100.0 | |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | 20% PEG6000, 0.1M bicine pH 9.0 |