6GBH
Helicobacter pylori adhesin HopQ type II bound to the N-terminal domain of human CEACAM1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 79.820, 169.670, 198.096 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.050 | 2.660 |
High resolution limit [Å] | 2.590 | 2.590 |
Rmerge | 0.123 | |
Rpim | 0.043 | |
Number of reflections | 42047 | 5934 |
<I/σ(I)> | 11.7 | 0.9 |
Completeness [%] | 99.6 | 97.3 |
Redundancy | 9.2 | 9 |
CC(1/2) | 0.999 | 0.605 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | Condition A4 of the JB Screen Classic HTS II screen (Jena Bioscience) (1 M Ammonium sulfate, 100 mM Tris; pH 8.5) |