6G0B
Crystal Structure of a GH8 xylotriose complex from Teredinibacter Turnerae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-04-18 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 59.721, 80.522, 87.986 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 59.470 - 1.800 |
| R-factor | 0.16831 |
| Rwork | 0.167 |
| R-free | 0.19743 |
| Starting model (for MR) | 6g00 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.511 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.470 | 1.840 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 40092 | |
| <I/σ(I)> | 8.5 | |
| Completeness [%] | 100.0 | |
| Redundancy | 7.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | 0.1 M sodium acetate, pH 5, 0.2 M ammonium sulfate, 20% PEG 6000 |
