6FX5
MITF dimerization mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-26 |
Detector | MARRESEARCH |
Wavelength(s) | 0.8726 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 38.720, 92.830, 86.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.045 - 2.050 |
R-factor | 0.2258 |
Rwork | 0.224 |
R-free | 0.24630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ath |
RMSD bond length | 0.017 |
RMSD bond angle | 1.385 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.045 | 2.160 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 9762 | 987 |
<I/σ(I)> | 7.8 | 3.5 |
Completeness [%] | 96.5 | 98 |
Redundancy | 3.8 | 3.8 |
CC(1/2) | 0.990 | 0.880 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | Crystals grew in conditions between 2.0 M and 2.4 M Ammonium sulfate and 0.1 and 0.15 M Cadmium Sulfate |