6FPR
Co-translational folding intermediate dictates membrane targeting of the signal recognition particle (SRP)- receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.953723 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 164.573, 35.487, 31.697 |
Unit cell angles | 90.00, 96.48, 90.00 |
Refinement procedure
Resolution | 19.930 - 2.650 |
R-factor | 0.24023 |
Rwork | 0.238 |
R-free | 0.27699 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qy9 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.597 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.880 | 2.790 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.092 | 0.545 |
Rmeas | 0.099 | 0.586 |
Number of reflections | 5435 | 781 |
<I/σ(I)> | 15.1 | 3.9 |
Completeness [%] | 99.7 | 100 |
Redundancy | 7.4 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 22% MPD NaCacodylate pH=6.2 |