Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-07-21 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.8726 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 119.556, 163.248, 177.625 |
| Unit cell angles | 90.00, 94.40, 90.00 |
Refinement procedure
| Resolution | 88.550 - 2.790 |
| R-factor | 0.207 |
| Rwork | 0.205 |
| R-free | 0.25220 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.570 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 95.550 | 2.840 |
| High resolution limit [Å] | 2.790 | 2.790 |
| Rmerge | 0.010 | 0.590 |
| Number of reflections | 167730 | |
| <I/σ(I)> | 14.7 | 1.4 |
| Completeness [%] | 99.4 | 89 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 800 MM SODIUM CITRATE, 100 MM IMIDAZOLE (PH 8.0) |
