6FMY
IMISX-EP of S-PepTSt
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-08-14 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 2.0664 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 101.220, 110.200, 111.470 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.290 - 2.700 |
| R-factor | 0.2102 |
| Rwork | 0.208 |
| R-free | 0.24610 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.705 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXCD |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.290 | 2.770 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmeas | 0.320 | 1.690 |
| Number of reflections | 33070 | 2441 |
| <I/σ(I)> | 40.2 | 8.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 423.6 | 378 |
| CC(1/2) | 1.000 | 0.960 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 293 | 22 %(v/v) PEG- 400, 325 mM ammonium dihydrogen phosphate, 100 mM HEPES, pH 7.0 |
