6FJQ

Adenovirus species 48, fiber knob protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-05-12
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9795
Spacegroup name	P 43 3 2
Unit cell lengths	145.205, 145.205, 145.205
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	83.830 - 2.910
R-factor	0.20525
Rwork	0.201
R-free	0.29134
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1knb
RMSD bond length	0.019
RMSD bond angle	2.293
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0189)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	83.820	2.990
High resolution limit [Å]	2.910	2.910
Rmerge	0.125	3.026
Rmeas	0.127	3.063
Number of reflections	12061	877
<I/σ(I)>	22.2
Completeness [%]	100.0	100
Redundancy	41.2	41.4
CC(1/2)	1.000	0.705

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	293	0.1 M Bis-Tris-propane, 20% PEG 3350, 0.2M NaNO3