6FDN

Rio2 structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	110
Detector technology	CCD
Collection date	2010-09-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9788
Spacegroup name	P 21 21 21
Unit cell lengths	58.592, 86.405, 121.544
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.300 - 2.900
R-factor	0.228
Rwork	0.226
R-free	0.26700
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.008
RMSD bond angle	1.030
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	BUSTER (2.10.3)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	70.420	3.070
High resolution limit [Å]	2.900	2.900
Rpim	0.041	0.354
Number of reflections	47430	4662
<I/σ(I)>	13.81	2.62
Completeness [%]	92.2	88.49
Redundancy	88.49	1.9
CC(1/2)	0.997	0.744

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	Morpheus D2