Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-10-02 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.607, 90.783, 75.378 |
| Unit cell angles | 90.00, 92.00, 90.00 |
Refinement procedure
| Resolution | 75.330 - 1.300 |
| R-factor | 0.17917 |
| Rwork | 0.178 |
| R-free | 0.19767 |
| Structure solution method | SAD |
| RMSD bond length | 0.032 |
| RMSD bond angle | 2.677 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | Auto-Rickshaw |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.330 | 1.330 |
| High resolution limit [Å] | 1.300 | 1.300 |
| Number of reflections | 164237 | |
| <I/σ(I)> | 19.9 | |
| Completeness [%] | 97.9 | 96.1 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 100 mM HEPES-Na pH 7.0, 1.0 M lithium sulphate |
