6F0S
Crystal structure of Pizza6-SYW
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ELETTRA BEAMLINE 5.2R |
| Synchrotron site | ELETTRA |
| Beamline | 5.2R |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-07-21 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 33.710, 69.910, 46.940 |
| Unit cell angles | 90.00, 107.23, 90.00 |
Refinement procedure
| Resolution | 32.197 - 1.500 |
| R-factor | 0.1764 |
| Rwork | 0.175 |
| R-free | 0.20370 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.994 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.200 | 1.530 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.060 | 0.328 |
| Rpim | 0.055 | 0.298 |
| Number of reflections | 33043 | |
| <I/σ(I)> | 11.1 | 3.3 |
| Completeness [%] | 99.1 | 98.7 |
| Redundancy | 3.4 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.2 M calcium chloride, 15% (w/v) PEG6000, and 0.1 M sodium acetate pH 5.0 |
