6EYX
Anti-CRISPR AcrIIa6 tetragonal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-22 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.370, 71.370, 177.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.380 - 1.960 |
R-factor | 0.2095 |
Rwork | 0.209 |
R-free | 0.22610 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.010 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.100 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmeas | 0.139 | 1.170 |
Number of reflections | 33785 | 5971 |
<I/σ(I)> | 15.8 | 3.5 |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 24 | 24 |
CC(1/2) | 0.998 | 0.880 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Magnesium chloride, 0.1M tris pH6.5-7.5, 5-15%(w/v) PEG 8000 |