6EUH
The GH43, Beta 1,3 Galactosidase, BT3683 with galactodeoxynojirimycin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 1 |
Unit cell lengths | 52.180, 77.200, 78.690 |
Unit cell angles | 114.00, 101.78, 100.78 |
Refinement procedure
Resolution | 68.190 - 2.000 |
R-factor | 0.18526 |
Rwork | 0.183 |
R-free | 0.22559 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.553 |
Data reduction software | HKL-2000 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 68.190 |
High resolution limit [Å] | 1.760 |
Number of reflections | 36549 |
<I/σ(I)> | 11.5 |
Completeness [%] | 99.9 |
Redundancy | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG 3350 0.2 M Ammonium Formate |