6ENO
Double cubane cluster oxidoreductase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 80.591, 80.591, 217.428 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.456 - 1.635 |
R-factor | 0.1738 |
Rwork | 0.172 |
R-free | 0.21330 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.202 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2621: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.900 |
High resolution limit [Å] | 1.630 |
Number of reflections | 51968 |
<I/σ(I)> | 13.9 |
Completeness [%] | 98.8 |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | PEG 8000, Na-citrate, Na-dithinite |