6EMG

Crystal structure of Rrp1 from Chaetomium thermophilum in space group P6322

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-05-01
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.99188
Spacegroup name	P 63 2 2
Unit cell lengths	214.259, 214.259, 124.785
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.222 - 2.240
R-factor	0.1882
Rwork	0.187
R-free	0.20690
Structure solution method	SAD
RMSD bond length	0.003
RMSD bond angle	0.643
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	SHELXDE
Refinement software	PHENIX (1.11.1_2575)

Data quality characteristics

	Overall
Low resolution limit [Å]	49.222
High resolution limit [Å]	2.240
Number of reflections	80956
<I/σ(I)>	24.62
Completeness [%]	100.0
Redundancy	20.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	291	0.8M K-H2PO4 0.8M Na-H2PO4