6EJJ
Structure of a glycosyltransferase / state 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 123 |
| Detector technology | PIXEL |
| Collection date | 2016-11-18 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.510, 125.780, 71.010 |
| Unit cell angles | 90.00, 90.28, 90.00 |
Refinement procedure
| Resolution | 29.814 - 2.700 |
| R-factor | 0.2082 |
| Rwork | 0.206 |
| R-free | 0.24440 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6eji |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.860 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.796 |
| High resolution limit [Å] | 2.300 | 2.700 |
| Rmerge | 0.212 | 1.743 |
| Number of reflections | 48793 | |
| <I/σ(I)> | 5.6 | 1.69 |
| Completeness [%] | 96.3 | 100 |
| Redundancy | 6.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | Ammonium acetate, ADA, PEG3350 |
