6EF9

GspB Siglec domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-G
Synchrotron site	APS
Beamline	21-ID-G
Temperature [K]	100
Detector technology	CCD
Collection date	2015-12-22
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.979
Spacegroup name	H 3 2
Unit cell lengths	92.083, 92.083, 143.928
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	33.219 - 1.300
R-factor	0.1313
Rwork	0.131
R-free	0.14380
RMSD bond length	0.008
RMSD bond angle	0.981
Refinement software	PHENIX ((1.12_2829))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.330
High resolution limit [Å]	1.300	1.300
Number of reflections	57769
<I/σ(I)>	59.3
Completeness [%]	99.9
Redundancy	13.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	4 M NaFormate