6EEX

L-GSTSTA from degenerate octameric repeats in InaZ, residues 707-712

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-01
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9791
Spacegroup name	P 21 21 21
Unit cell lengths	9.210, 11.980, 22.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	11.400 - 1.100
R-factor	0.0622
Rwork	0.061
R-free	0.06880
Structure solution method	AB INITIO PHASING
RMSD bond length	0.007
RMSD bond angle	1.547
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHELXD
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	11.400	11.400	1.150
High resolution limit [Å]	1.100	3.650	1.100
Rmerge	0.125	0.066	0.219
Rmeas	0.136	0.075	0.243
Number of reflections	1093	45	117
<I/σ(I)>	10.41	13.01	7.34
Completeness [%]	91.7	95.7	74.5
Redundancy	6.476	4.8	6.427
CC(1/2)	0.988	0.999	0.979

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9.5	298	0.1M CHES pH 9.5, 10% (w/v) of PEG 3000