6DZ6
Structure of the Orthorhombic (Orthrhmb) Crystal Form of Human Apolipoprotein C1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-08-15 |
| Detector | SDMS |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 34.459, 53.698, 71.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.000 - 3.000 |
| R-factor | 0.22702 |
| Rwork | 0.224 |
| R-free | 0.28270 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.546 |
| Data reduction software | DENZO |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.000 | 3.180 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.169 | 0.491 |
| Rmeas | 0.180 | 0.619 |
| Rpim | 0.080 | 0.369 |
| Number of reflections | 2687 | 180 |
| <I/σ(I)> | 5.5 | 1.1 |
| Completeness [%] | 91.8 | 56.3 |
| Redundancy | 7.1 | 1.7 |
| CC(1/2) | 0.997 | 0.733 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 298 | 16% MPD - 18% MPD |
