6DLE
Crystal structure of IgLON5 homodimer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F1 |
| Synchrotron site | CHESS |
| Beamline | F1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.98 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 119.205, 138.234, 160.836 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.895 - 3.994 |
| R-factor | 0.2649 |
| Rwork | 0.260 |
| R-free | 0.30780 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6dld |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.634 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.895 | 4.230 |
| High resolution limit [Å] | 3.994 | 4.000 |
| Number of reflections | 11556 | |
| <I/σ(I)> | 7.12 | |
| Completeness [%] | 99.3 | |
| Redundancy | 6.6 | |
| CC(1/2) | 0.995 | 0.336 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | Na,K-Tartrate, BTP pH 7.0 |
