Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1996-01-20 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 124.000, 102.500, 167.302 |
| Unit cell angles | 90.00, 101.64, 90.00 |
Refinement procedure
| Resolution | 28.594 - 2.500 |
| R-factor | 0.2029 |
| Rwork | 0.202 |
| R-free | 0.24630 |
| Structure solution method | SIR |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.663 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MLPHARE |
| Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.000 | 2.589 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 127922 | |
| <I/σ(I)> | 11 | |
| Completeness [%] | 88.0 | |
| Redundancy | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | sodium chloride, b-octylglucopyranoside, PEG8000, MPD, sodium azide, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
