6D3B
INFLUENZA VIRUS NEURAMINIDASE SUBTYPE N9 (TERN) APO FORM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95369 |
Spacegroup name | I 4 3 2 |
Unit cell lengths | 180.994, 180.994, 180.994 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.070 - 1.400 |
R-factor | 0.15261 |
Rwork | 0.152 |
R-free | 0.16982 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7nn9 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.938 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.070 | 1.440 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.122 | 0.873 |
Number of reflections | 92499 | |
<I/σ(I)> | 29.8 | 1.79 |
Completeness [%] | 99.0 | 99.6 |
Redundancy | 26 | 14.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 1.4 M KH2PO4 + 3.0 M K2HPO4 (2:1) |