6CKB
Crystal structure of an extended beta3 integrin P33
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-08-19 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.97872 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.080, 80.910, 126.720 |
Unit cell angles | 90.00, 96.36, 90.00 |
Refinement procedure
Resolution | 58.700 - 2.800 |
R-factor | 0.2422 |
Rwork | 0.239 |
R-free | 0.29640 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.052 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.700 | 2.890 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 29474 | |
<I/σ(I)> | 8.6 | |
Completeness [%] | 100.0 | |
Redundancy | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 20% PEG 6000, 0.1 M Tris-HCl (pH 8.5) |