6CJS
Candida albicans Hsp90 nucleotide binding domain in complex with AUY922
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2017-11-18 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.03319 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 86.210, 86.210, 225.846 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.100 - 1.900 |
Rwork | 0.167 |
R-free | 0.19340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6cji |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.100 | 1.960 |
High resolution limit [Å] | 1.890 | 1.890 |
Rmerge | 0.081 | |
Number of reflections | 34601 | 3371 |
<I/σ(I)> | 16.9 | 1.2 |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 12.9 | 12.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298.15 | 0.1M Hepes 0.02M MgCl2 22% Polyacrylic acid sodium salt 5100 |