6CIW

Hen Egg White Lysozyme Cocrystallized with 1,3-Di(2-pyridyl)propane

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SEALED TUBE
Source details	BRUKER IMUS MICROFOCUS
Temperature [K]	100
Detector technology	CCD
Collection date	2017-11-28
Detector	APEX II CCD
Wavelength(s)	1.4200
Spacegroup name	P 43 21 2
Unit cell lengths	76.874, 76.874, 37.249
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.360 - 1.420
R-factor	0.2421
Rwork	0.240
R-free	0.27640
RMSD bond length	0.020
RMSD bond angle	2.083
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0151)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	54.360	1.461
High resolution limit [Å]	1.420	1.424
Number of reflections	21208
<I/σ(I)>	1
Completeness [%]	99.0
Redundancy	1.001

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	0.1 M sodium acetate pH 5.0 1M NaCl