6BYB
Crystal structure of L3MBTL1 MBT Domain with MBK14970
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-23 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 85.880, 93.166, 58.444 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.000 - 1.740 |
R-factor | 0.2014 |
Rwork | 0.200 |
R-free | 0.22160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rjd |
RMSD bond length | 0.010 |
RMSD bond angle | 1.425 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.6.1) |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.770 |
High resolution limit [Å] | 1.740 | 4.720 | 1.740 |
Rmerge | 0.075 | 0.035 | 0.748 |
Rmeas | 0.082 | 0.039 | 0.841 |
Rpim | 0.031 | 0.015 | 0.376 |
Total number of observations | 325154 | ||
Number of reflections | 48892 | 2632 | 2336 |
<I/σ(I)> | 10.7 | ||
Completeness [%] | 99.8 | 98.8 | 97.3 |
Redundancy | 6.7 | 6.2 | 4.7 |
CC(1/2) | 0.999 | 0.650 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 30% PEG 400, 0.2 M Magnesium chloride hexahydrate, 0.1 M Sodium HEPES pH7.5 |