6BWZ
SYSGYS from low-complexity domain of FUS, residues 37-42
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 17.569, 4.818, 18.283 |
Unit cell angles | 90.00, 91.03, 90.00 |
Refinement procedure
Resolution | 18.280 - 1.100 |
R-factor | 0.1434 |
Rwork | 0.141 |
R-free | 0.16460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3nvh |
RMSD bond length | 0.014 |
RMSD bond angle | 1.799 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.5.6) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 1.140 |
High resolution limit [Å] | 1.100 | 2.370 | 1.100 |
Rmerge | 0.179 | 0.114 | 0.468 |
Total number of observations | 5560 | ||
Number of reflections | 1182 | ||
<I/σ(I)> | 6.5 | ||
Completeness [%] | 82.0 | 89.5 | 28.4 |
Redundancy | 4.7 | 4.4 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 0.1M Bis-Tris pH 6.0, 0.2M Magnesium Formate Dihydrate |