Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-12-01 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.206, 92.555, 128.698 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.278 - 2.780 |
| R-factor | 0.2191 |
| Rwork | 0.217 |
| R-free | 0.29860 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.462 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 46.278 | 46.278 | 3.030 |
| High resolution limit [Å] | 2.780 | 17.790 | 2.780 |
| Rmerge | 0.046 | 0.016 | 0.435 |
| Rmeas | 0.053 | 0.019 | 0.506 |
| Total number of observations | 92390 | ||
| Number of reflections | 25234 | 111 | 5670 |
| <I/σ(I)> | 18.67 | 64.56 | 3.15 |
| Completeness [%] | 96.0 | 88.8 | 96.4 |
| Redundancy | 3.661 | 3.441 | 3.76 |
| CC(1/2) | 0.999 | 1.000 | 0.919 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298 | 16% PEG 8K, 0.2 M NH4 acetate, 0.1 M CHES pH 8.75 |
