6ARD
Monoclinic EutL - structure determined from merged "Group 2" data
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-E |
| Synchrotron site | APS |
| Beamline | 24-ID-E |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-10-28 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9791 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.720, 66.140, 78.580 |
| Unit cell angles | 90.00, 111.22, 90.00 |
Refinement procedure
| Resolution | 19.650 - 2.000 |
| R-factor | 0.1807 |
| Rwork | 0.179 |
| R-free | 0.21740 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4edi |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.534 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((dev_2686: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.110 | 2.080 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 35264 | |
| <I/σ(I)> | 8.66 | 1.73 |
| Completeness [%] | 91.5 | 93.6 |
| Redundancy | 4.56 | 1.65 |
| CC(1/2) | 0.992 | 0.718 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 298 | 0.1M sodium potassium phosphate, 0.25 sodium chloride, 10% PEG 8000 |
