6ABZ
Crystal Structure of HEWL in deionized water
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-01 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9792 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 78.139, 78.139, 37.140 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 55.250 - 1.700 |
| R-factor | 0.17433 |
| Rwork | 0.171 |
| R-free | 0.23415 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dpx |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.895 |
| Data reduction software | iMOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.250 | 1.790 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.200 | |
| Number of reflections | 13065 | |
| <I/σ(I)> | 9.2 | |
| Completeness [%] | 99.3 | |
| Redundancy | 10.14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 292 | 0.1 M sodium acetate pH 4.6 and 2 M NaCl |
