6A65

Placental protein 13/galectin-13 variant R53HR55N with Tris

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.977
Spacegroup name	C 2 2 2
Unit cell lengths	57.316, 91.699, 50.339
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.911 - 1.771
R-factor	0.2061
Rwork	0.201
R-free	0.25400
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.911	1.810
High resolution limit [Å]	1.770	1.770
Number of reflections	13108
<I/σ(I)>	15.7
Completeness [%]	98.7
Redundancy	1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG