6A09

Salmonella Typhi YfdX in the P222 space group

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	93
Detector technology	CCD
Collection date	2016-05-04
Detector	ADSC QUANTUM 270
Wavelength(s)	1.000
Spacegroup name	P 2 2 2
Unit cell lengths	72.395, 127.071, 170.384
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.505 - 2.293
R-factor	0.1815
Rwork	0.180
R-free	0.23340
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6a02
RMSD bond length	0.007
RMSD bond angle	0.839
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.340
High resolution limit [Å]	2.293	2.300
Rpim	0.035	0.144
Number of reflections	70194	3229
<I/σ(I)>	29.5
Completeness [%]	98.5
Redundancy	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5	293	4% Tacsimate (pH 5.0), 12% PEG3350