5YB2
Crystal structure of LP-11/N44
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-11-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9796 |
Spacegroup name | H 3 |
Unit cell lengths | 110.884, 110.884, 125.382 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.720 - 3.800 |
R-factor | 0.2841 |
Rwork | 0.283 |
R-free | 0.30680 |
Structure solution method | MOLECULAR REPLACEMENT |
Data scaling software | HKL-2000 (V1.0) |
Phasing software | PHASER (7.0) |
Refinement software | PHENIX (1.10.1-2155-000) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 27.720 |
High resolution limit [Å] | 3.800 |
Number of reflections | 5647 |
<I/σ(I)> | 14.4 |
Completeness [%] | 100.0 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.1 M HEPES pH 7.5, 2.0 M Ammonium sulfate |