5XLZ
The crystal structure of tubulin complexed with a benzylidene derivative of 9(10H)-anthracenone
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17B1 |
Synchrotron site | SSRF |
Beamline | BL17B1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 105.465, 158.439, 181.600 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 42.668 - 2.298 |
R因子 | 0.2165 |
Rwork | 0.216 |
R-free | 0.24660 |
結合長の平均二乗偏差(RMSD) [Å] | 0.003 |
結合角の平均二乗偏差(RMSD) [度] | 0.828 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 50.000 |
分解能 [Å] (高) | 2.298 |
独立反射数 | 135594 |
<I/σ(I)> | 15.5 |
完全性 [%] | 99.8 |
冗長性 | 6.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 6% poly(ethylene glycol) 4000, 8% glycerol, 0.1M Mes, 30mM CaCl2, 30mM MgCl2, pH 6.7 |