5TDW
Set3 PHD finger in complex with histone H3K4me3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-02 |
Detector | NOIR-1 |
Wavelength(s) | 1.00 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 25.870, 43.680, 85.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.530 - 1.700 |
R-factor | 0.1662 |
Rwork | 0.165 |
R-free | 0.19910 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.134 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.540 |
High resolution limit [Å] | 1.700 |
Number of reflections | 11089 |
<I/σ(I)> | 14 |
Completeness [%] | 99.9 |
Redundancy | 26.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 273 | 20% PEG3350, 0.2 M sodium citrate |