5MWX
Galectin-1 in Complex with Ligand JB60
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-12 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97242 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.260, 58.250, 111.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.319 - 1.290 |
R-factor | 0.1706 |
Rwork | 0.169 |
R-free | 0.20490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.023 |
RMSD bond angle | 1.653 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (dev_2443) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.320 |
High resolution limit [Å] | 1.290 |
Number of reflections | 71546 |
<I/σ(I)> | 11.71 |
Completeness [%] | 99.0 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 1.5 M AMMONIUM SULFATE, PH 7.5 |