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5MDH

CRYSTAL STRUCTURE OF TERNARY COMPLEX OF PORCINE CYTOPLASMIC MALATE DEHYDROGENASE ALPHA-KETOMALONATE AND TNAD AT 2.4 ANGSTROMS RESOLUTION

Experimental procedure
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX7.2
Synchrotron siteSRS
BeamlinePX7.2
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1996-08
DetectorMARRESEARCH
Spacegroup nameP 21 21 2
格子定数 [Å]85.700, 144.432, 59.226
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基15.000 - 2.400
R因子0.199

*

Rwork0.199
R-free0.25378

*

Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4mdh
結合長の平均二乗偏差(RMSD) [Å]0.010
結合角の平均二乗偏差(RMSD) [度]0.034
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareREFMAC
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)15.0002.510
分解能 [Å] (高)2.4002.400
Rmerge_l_obs0.0930.320
独立反射数26268
<I/σ(I)>12.343.72
完全性 [%]89.391.6
冗長性3.963.9
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

*

5.6pH 5.6
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11reservoirammonium acetate0.15 (mM)
21reservoirPEG400016 (%(v/v))

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件を2024-09-18に公開中

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