5J9Q
Crystal structure of the NuA4 core complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2014-01-10 |
Detector | ADSC QUANTUM 4r |
Wavelength(s) | 0.987 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 217.857, 190.990, 172.346 |
Unit cell angles | 90.00, 113.56, 90.00 |
Refinement procedure
Resolution | 29.996 - 3.250 |
R-factor | 0.2508 |
Rwork | 0.250 |
R-free | 0.27310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.621 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | autoSHARP |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 3.250 |
Number of reflections | 79960 |
<I/σ(I)> | 6.9 |
Completeness [%] | 79.6 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 289 | 100mM NaCitrate (pH 6.5), 1.79M ammonium sulfate, 5%(w/v) glycerol |