5HS4
Plasmdoium Vivax Lactate dehydrogenase
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-27 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9796 |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 75.792, 80.613, 93.377 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 23.765 - 1.339 |
R因子 | 0.151 |
Rwork | 0.150 |
R-free | 0.17140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2a92 |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.163 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 25.000 | 25.000 | 1.360 |
分解能 [Å] (高) | 1.339 | 3.630 | 1.340 |
Rmerge_l_obs | 0.076 | 0.051 | 0.274 |
独立反射数 | 63845 | ||
<I/σ(I)> | 19.4 | ||
完全性 [%] | 99.2 | 97.1 | 97.3 |
冗長性 | 11.8 | 13.5 | 8.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | ammonium nitrate, PEG-3350, magnesium ion, potassium chloride |