5FT0
Crystal structure of gp37(Dip) from bacteriophage phiKZ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-04-17 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.040, 65.020, 85.400 |
Unit cell angles | 90.00, 107.68, 90.00 |
Refinement procedure
Resolution | 46.025 - 2.200 |
R-factor | 0.1952 |
Rwork | 0.194 |
R-free | 0.21890 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.004 |
RMSD bond angle | 0.655 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHENIX (AUTOSOLVE) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.600 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.110 | 0.810 |
Number of reflections | 38346 | |
<I/σ(I)> | 8.2 | 2.1 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 5.2 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 100 MM KH2PO4, 100 MM NAH2PO4, 100 MM MES PH 6.0, 800 MM NACL, 0.2 M SODIUM THIOCYANATE |