5C8H
Crystal structure of ORC2 C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792604 |
Spacegroup name | P 61 |
Unit cell lengths | 55.038, 55.038, 75.629 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.660 - 2.010 |
R-factor | 0.196 |
Rwork | 0.190 |
R-free | 0.25730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | polyalanine coordinates derived from PDB entry 4XGC. |
RMSD bond length | 0.015 |
RMSD bond angle | 1.499 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.7) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0123) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.660 | 47.660 | 2.060 |
High resolution limit [Å] | 2.010 | 9.000 | 2.010 |
Rmerge | 0.077 | 0.030 | 1.030 |
Rpim | 0.024 | 0.009 | 0.327 |
Total number of observations | 96076 | 1011 | 6717 |
Number of reflections | 8700 | ||
<I/σ(I)> | 21.5 | 63.8 | 2.2 |
Completeness [%] | 99.8 | 98.8 | 98.1 |
Redundancy | 11 | 9.4 | 10.6 |
CC(1/2) | 0.999 | 0.999 | 0.801 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG-3350, 0.2 M magnesium formate |