5B5R
Crystal structure of GSDMA3
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2015-09-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97776 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 43.453, 103.414, 49.625 |
格子定数 [度] | 90.00, 110.57, 90.00 |
精密化法
残基 | 37.914 - 1.902 |
R因子 | 0.1893 |
Rwork | 0.187 |
R-free | 0.23200 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.848 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.930 |
分解能 [Å] (高) | 1.900 | 1.900 |
Rmerge_l_obs | 0.071 | 0.876 |
独立反射数 | 44110 | |
<I/σ(I)> | 25.6 | 2.4 |
完全性 [%] | 97.1 | 92.7 |
冗長性 | 6.6 | 5.1 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 100 mM Bis-Tris (pH 6.5), 19% polyethylene glycol 3550, 10 mM TCEP |