5ZW6
Structure of spAimR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-07-11 |
| Detector | DECTRIS PILATUS3 R 1M |
| Wavelength(s) | 0.97776 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 150.795, 193.576, 33.321 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.024 - 2.050 |
| R-factor | 0.1924 |
| Rwork | 0.190 |
| R-free | 0.23450 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.929 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.024 | 2.120 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Number of reflections | 62871 | |
| <I/σ(I)> | 1.3 | |
| Completeness [%] | 100.0 | 99.98 |
| Redundancy | 18.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4 | 293 | 20% PEG 3350, 0.1 M sodium citrate pH 4.0, 0.2 M Citric Acid |
