Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL15A1 |
| Synchrotron site | NSRRC |
| Beamline | BL15A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-18 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 1.60572, 1.56518, 1.60490 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 38.299, 38.299, 54.328 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 12.444 - 1.660 |
| R-factor | 0.235638826004 |
| Rwork | 0.233 |
| R-free | 0.25530 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.692 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXS |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.720 |
| High resolution limit [Å] | 1.660 | 1.660 |
| Rmerge | 0.048 | 0.272 |
| Number of reflections | 3447 | 632 |
| <I/σ(I)> | 41.724 | |
| Completeness [%] | 96.1 | |
| Redundancy | 5.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277.15 | 50mM Sodium cacodylate, 1mM Magnesium chloride, 5% MPD, 2mM Cobalt(II) chloride, 1mM Chromomycin A3 |
