5ZQ6
SidE-Ubi-ADPr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2017-12-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 92.322, 128.003, 191.065 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.943 - 3.009 |
R-factor | 0.1828 |
Rwork | 0.180 |
R-free | 0.23160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zq5 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.987 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.100 |
High resolution limit [Å] | 3.000 | 3.010 |
Rmerge | 0.177 | |
Rmeas | 0.191 | |
Rpim | 0.070 | 0.399 |
Number of reflections | 45143 | |
<I/σ(I)> | 12.6 | |
Completeness [%] | 99.9 | |
Redundancy | 7.2 | |
CC(1/2) | 0.795 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, Tacsimate |