5ZLQ

Crystal Structure of C1orf123

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B2
Synchrotron site	SPring-8
Beamline	BL26B2
Temperature [K]	100
Detector technology	CCD
Collection date	2015-07-01
Detector	RAYONIX MX225HE
Wavelength(s)	1.0
Spacegroup name	I 2 3
Unit cell lengths	118.131, 118.131, 118.131
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.690 - 2.000
R-factor	0.1831
Rwork	0.180
R-free	0.23300
Structure solution method	SAD
RMSD bond length	0.020
RMSD bond angle	1.937
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AutoSol
Refinement software	REFMAC (5.8.0189)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.030
High resolution limit [Å]	2.000	5.430	2.000
Rmerge	0.067	0.026	0.727
Rmeas	0.067	0.027	0.735
Rpim	0.010	0.004	0.113
Number of reflections	18717	987	915
<I/σ(I)>	13
Completeness [%]	99.9	98.2	100
Redundancy	44.2	41.6	42.1
CC(1/2)		1.000	0.975

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	4.5	293	Ammonium sulfate, Sodium acetate