5ZKE

Crystal Structure of N-terminal Domain of Plasmodium vivax p43 in space group P212121

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-05-05
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9763
Spacegroup name	P 21 21 21
Unit cell lengths	59.146, 74.618, 77.452
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.309 - 1.492
R-factor	0.1472
Rwork	0.146
R-free	0.17060
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	53.740	1.497
High resolution limit [Å]	1.492	1.492
Number of reflections	56387
<I/σ(I)>	18.9
Completeness [%]	99.9	96.7
Redundancy	13	13.4
CC(1/2)	1.000	0.800

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.2M sodium citrate, 20 % w/v PEG 3350