5Z5K

Structure of the DCC-Draxin complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-08-15
Detector	ADSC QUANTUM 315r
Wavelength(s)	1
Spacegroup name	P 65
Unit cell lengths	108.069, 108.069, 130.266
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	35.374 - 2.493
R-factor	0.2143
Rwork	0.212
R-free	0.24750
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.581
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.540
High resolution limit [Å]	2.493	6.780	2.500
Rmerge	0.102	0.055
Rmeas	0.107	0.058
Rpim	0.036	0.018	0.485
Number of reflections	29938
<I/σ(I)>	12.6
Completeness [%]	99.8	98.6	100
Redundancy	10.9	10.7	10.6
CC(1/2)		0.997	0.798

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG 3350, KCl